tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

Base Information

Chemical Name:tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate
CAS No.:1071817-57-6
Molecular Formula:C₁₈H₂₆O₉
Molecular Weight:386.399
Hs Code.:

Synonyms:tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

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Chemical Property of tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

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Technology Process of tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

There total 1 articles about tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1071817-58-7
tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)cyclohexa-2,5-dienecarboxylate

: 1071817-57-6
tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

Guidance literature:: With tert.-butylhydroperoxide; dipyridinium dichromate; Celite; In decane; benzene; at 20 ℃; for 4h;
DOI:10.1021/jo8015192

Reference yield:

: 1071817-57-6
tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate

: 78-80-8
2-methylbut-1-en-3-yne

: tert-butyl 4-hydroxy-1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-(3-methylbut-3-en-1-ynyl)cyclohexa-2,5-dienecarboxylate

Guidance literature:: 2-methylbut-1-en-3-yne; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 1h;

tert-butyl 1-[(methoxycarbonyl)methyl]-2,5-bis(methoxymethoxy)-4-oxocyclohexa-2,5-dienecarboxylate; In diethyl ether; hexane; for 3h;

With water; ammonium chloride; In diethyl ether; hexane;
DOI:10.1021/jo8015192