2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

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Chemical Name:2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid
CAS No.:1364369-10-7
Molecular Formula:C₃₄H₃₇N₅O₈
Molecular Weight:643.696
Hs Code.:

Synonyms:2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

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Chemical Property of 2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

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Technology Process of 2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

There total 8 articles about 2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1364369-21-0
tert-butyl 2-(2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenylazo)benzoate

: 1364369-10-7
2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1039/c2cc17542h

Reference yield:

: 1364369-16-3
methyl 4-(3-hydroxyphenoxy)butanoate

: 1364369-10-7
2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C

1.2: 0 - 20 °C

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

3.1: trifluoroacetic acid / dichloromethane / 16 h / 0 - 20 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; trifluoroacetic acid; sodium nitrite; In dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c2cc17542h

Reference yield:

: C₈H₇NO₃

: 1364369-10-7
2-((2-(4-(3-(7-(diethylamino)-2-oxo-2H-chromene-3-carboxamido)propylamino)-4-oxobutoxy)-4-hydroxyphenyl)diazenyl)benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 15 h / 20 °C

1.2: 2 h / 20 °C

2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C

2.2: 0 - 20 °C

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 3 h / 0 - 20 °C

4.1: trifluoroacetic acid / dichloromethane / 16 h / 0 - 20 °C

With hydrogenchloride; dmap; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium nitrite; In dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c2cc17542h