BENZYL 2-ACETAMIDO-3,6-DI-O-BENZOYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: BENZYL 2-ACETAMIDO-3,6-DI-O-BENZOYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE
• CAS No.: 82827-77-8
• Molecular Formula: C29H29 N O8
• Molecular Weight: 519.54
• Mol file: 82827-77-8.mol

Synonyms:N-Benzyl 2-Acetamido-3,6-di-O-benzoyl-2-deoxy-a-D-glucopyranoside

Chemical Property of BENZYL 2-ACETAMIDO-3,6-DI-O-BENZOYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

Chemical Property:

• Melting Point: 159-160°C
• PSA: 120.39000
• LogP: 3.26720

Purity/Quality:

98%Min ^*data from raw suppliers

Benzyl2-Acetamido-3,6-di-O-benzoyl-2-deoxy-α-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL 2-ACETAMIDO-3,6-DI-O-BENZOYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE

There total 3 articles about BENZYL 2-ACETAMIDO-3,6-DI-O-BENZOYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

benzoyl chloride (98-88-4) + benzyl 2-acetamido-3-O-benzoyl-2-deoxy-α-D-glucopyranoside (33423-31-3) → Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid (82827-77-8)

Guidance literature:

With pyridine; at -10 ℃; for 10h;

DOI:10.1016/S0008-6215(00)80689-8

Reference yield: 76.9%

benzoyl chloride (98-88-4) + benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside (13343-62-9,347411-88-5) → Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid (82827-77-8)

Guidance literature:

With pyridine; at 20 ℃; for 11h;

DOI:10.1016/S0008-6215(99)00314-6

Reference yield: 9.4%

1-benzoylimidazole (10364-94-0) + benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside (13343-62-9,347411-88-5) → Benzyl-2-acetamido-2-desoxy-3,6-di-O-dibenzoyl-α-D-glucopyranosid (82827-77-8) + benzyl 2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-α-D-glucopyranoside

Guidance literature:

In acetonitrile; for 17h; Heating;

DOI:10.1021/jo951934m

upstream raw materials:

benzoyl chloride

benzyl 2-acetamido-3-O-benzoyl-2-deoxy-α-D-glucopyranoside

benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside

1-benzoylimidazole

Downstream raw materials:

Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-(trifluormethylsulfonyl)-α-D-glucopyranosid

benzyl 2-acetamido-3,6-di-O-benzoyl-4-chloro-2,4-dideoxy-α-D-galactopyranoside

Benzyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-4-O-phenoxythiocarbonyl-α-D-glucopyranosid

benzyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-(2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl)-α-D-glucopyranoside

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