succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

Base Information

Chemical Name:succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate
CAS No.:372987-12-7
Molecular Formula:C₃₃H₃₆N₂O₁₀
Molecular Weight:620.656
Hs Code.:

Synonyms:succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

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Chemical Property of succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

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Technology Process of succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

There total 4 articles about succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 372987-03-6
(3S,4R,5S,6S)-3,6-Bis-benzyloxymethyl-1,8-diphenyl-octane-4,5-diol

: 372987-12-7
succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 2.29 g / (+/-)-camphor-10-sulfonic acid / acetone / 0.5 h

2: 1.27 g / H₂; NaHCO₃ / Pd/C / ethyl acetate; H₂O / 63 h / 20 °C

3: RuCl₃; NaIO₄ / acetonitrile; CH₂Cl₂; H₂O / 1.92 h

4: 393 mg / pyridine / acetonitrile

With pyridine; ruthenium trichloride; sodium periodate; camphor-10-sulfonic acid; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In dichloromethane; water; ethyl acetate; acetone; acetonitrile;
DOI:10.1021/jm0011171

Reference yield:

: 372987-07-0
(4S,5R)-4,5-Bis-((S)-1-benzyloxymethyl-3-phenyl-propyl)-2,2-dimethyl-[1,3]dioxolane

: 372987-12-7
succinimidyl (2R)-2-[(4R,5S)-5-(3-phenylpropyl-(1R)-1-succinimidyloxycarbonyl)-2,2-dimethyl-1,3-dioxolan-4-yl]-4-phenylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.27 g / H₂; NaHCO₃ / Pd/C / ethyl acetate; H₂O / 63 h / 20 °C

2: RuCl₃; NaIO₄ / acetonitrile; CH₂Cl₂; H₂O / 1.92 h

3: 393 mg / pyridine / acetonitrile

With pyridine; ruthenium trichloride; sodium periodate; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/jm0011171