trans-(triphenylphosphine)2Pt(CF₃)OH

Base Information

Chemical Name:trans-(triphenylphosphine)2Pt(CF₃)OH
CAS No.:71588-93-7
Molecular Formula:C₃₇H₃₁F₃OP₂Pt
Molecular Weight:805.675
Hs Code.:

trans-(triphenylphosphine)2Pt(CF<sub>3</sub>)OH

Synonyms:trans-(triphenylphosphine)2Pt(CF₃)OH

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Chemical Property of trans-(triphenylphosphine)2Pt(CF₃)OH

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Technology Process of trans-(triphenylphosphine)2Pt(CF₃)OH

There total 1 articles about trans-(triphenylphosphine)2Pt(CF₃)OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ((C₆H₅)3P)2Pt(CF₃)(COOH)

: 7722-84-1
dihydrogen peroxide

: 71588-93-7
trans-(triphenylphosphine)2Pt(CF₃)OH

Guidance literature:: In tetrahydrofuran; byproducts: CO2, trans-((C6H5)3P)2Pt(CF3)(OOH); (N2); added 34% H2O2 to a stirred suspn. of Pt-complex thermostated at 0°C; 20 h; concentrated; added diethyl ether; filtered;
DOI:10.1021/om00049a021

Reference yield: 93.0%

: 71581-10-7
trans-bis(triphenylphosphino)Pt(CF₃)Cl

: 71588-93-7
trans-(triphenylphosphine)2Pt(CF₃)OH

: 119296-26-3
{(bis(diphenylphosphino)methane)Pt(CF₃)P(C₆H₅)3}OH

Guidance literature:: In hexane; toluene; (N2); to suspn. of Pt complex in toluene/hexane (1:1) was added toluene soln. of ligand and stirred overnight; crude product was filtered off, washed with hexane and dried; recrystn. from CH2Cl2/hexane; elem. anal.;

Reference yield: 70.0%

: 71588-93-7
trans-(triphenylphosphine)2Pt(CF₃)OH

: ((C₆H₅)3P)2Pt(CF₃)(COOH)

Guidance literature:: With carbon monoxide; In toluene; (N2); saturated a soln. of Pt-complex with CO under stirring; stirred at room temp. for 5 h; concentrated; added hexane; pptd.; filtered; washed with hexane; dried; recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1021/om00049a021