N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

Base Information

Chemical Name:N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide
CAS No.:1365546-78-6
Molecular Formula:C₁₉H₁₉BrN₄O
Molecular Weight:399.29
Hs Code.:

Synonyms:N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

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Technology Process of N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

There total 2 articles about N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1131-18-6
1-Phenyl-3-methyl-5-aminopyrazole

: 1365546-78-6
N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 12 h / 20 °C

2: N-Bromosuccinimide / acetonitrile / 3 h / Reflux

With N-Bromosuccinimide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jo300176f

Reference yield:

: 78554-86-6
N-methyl-p-anisylimidoyl chloride

: 1365546-78-6
N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 12 h / 20 °C

2: N-Bromosuccinimide / acetonitrile / 3 h / Reflux

With N-Bromosuccinimide; triethylamine; In 1,4-dioxane; acetonitrile;
DOI:10.1021/jo300176f

Reference yield: 92.0%

: 1365546-78-6
N'-(4-bromo-3-methyl-1-phenyl-1H-pyrazol-5-yl)-4-methoxy-N-methylbenzimidamide

: 1365547-08-5
5-(4-methoxyphenyl)-3,4-dimethyl-1-phenyl-1,4-dihydroimidazo[4,5-c]pyrazole

Guidance literature:: With copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine; In N,N-dimethyl-formamide; for 8h; Inert atmosphere; Heating;
DOI:10.1021/jo300176f