N-methyl-p-anisylimidoyl chloride

Base Information Edit

Chemical Name:N-methyl-p-anisylimidoyl chloride
CAS No.:78554-86-6
Molecular Formula:C₉H₁₀ClNO
Molecular Weight:183.637
Hs Code.:
Mol file:78554-86-6.mol

Synonyms:N-methyl-p-anisylimidoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-p-anisylimidoyl chloride Edit

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Technology Process of N-methyl-p-anisylimidoyl chloride

There total 2 articles about N-methyl-p-anisylimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 3400-22-4
4-methoxy-N-methylbenzamide

: 78554-86-6
N-methyl-p-anisylimidoyl chloride

Guidance literature:: With thionyl chloride; Heating;
DOI:10.1021/jo00177a032

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 78554-86-6
N-methyl-p-anisylimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: thionyl chloride / 20 °C

With thionyl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1039/c3cc41690a