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Technology Process of [N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

[N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

Base Information
  • Chemical Name:[N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]
  • CAS No.:155941-76-7
  • Molecular Formula:C8H20N*C12H11Cl3O2Re
  • Molecular Weight:610.038
  • Hs Code.:
[N(C<sub>2</sub>H<sub>5</sub>)4]<sup>(1+)</sup>*[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]<sup>(1-)</sup>=[N(C<sub>2</sub>H<sub>5</sub>)4][Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]

Synonyms:[N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

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Chemical Property of [N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]
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Technology Process of [N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

There total 1 articles about [N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)4(SO<sub>3</sub>CF<sub>3</sub>)]<sup>(1+)</sup>*SO<sub>3</sub>CF<sub>3</sub><sup>(1-)</sup>=[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)4(SO<sub>3</sub>CF<sub>3</sub>)]SO<sub>3</sub>CF<sub>3</sub>
155941-74-5

[Re(CC6H2(CH3)3)(CO)4(SO3CF3)](1+)*SO3CF3(1-)=[Re(CC6H2(CH3)3)(CO)4(SO3CF3)]SO3CF3

tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

[N(C<sub>2</sub>H<sub>5</sub>)4]<sup>(1+)</sup>*[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]<sup>(1-)</sup>=[N(C<sub>2</sub>H<sub>5</sub>)4][Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]
155941-76-7

[N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

Guidance literature:
In dichloromethane; byproducts: CO, tetraethylammonium triflate; reaction under inert gas: addn. of (NEt4)Cl to a slurry of Re-complex in CH2Cl2, stirring for 4 h; removal of solvent, product could not be separated from (NEt4)OTf;
DOI:10.1021/om00017a080

Reference yield: 65.0%

thallium(I) tetrafluoroborate
28625-02-7

thallium(I) tetrafluoroborate

[N(C<sub>2</sub>H<sub>5</sub>)4]<sup>(1+)</sup>*[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]<sup>(1-)</sup>=[N(C<sub>2</sub>H<sub>5</sub>)4][Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>3</sub>]
155941-76-7

[N(C2H5)4](1+)*[Re(CC6H2(CH3)3)(CO)2Cl3](1-)=[N(C2H5)4][Re(CC6H2(CH3)3)(CO)2Cl3]

[Re(CC<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)(CO)2Cl<sub>2</sub>(C<sub>5</sub>H<sub>5</sub>N)]
155941-77-8

[Re(CC6H2(CH3)3)(CO)2Cl2(C5H5N)]

Guidance literature:
With pyridine; In pyridine; byproducts: TlCl; reaction under inert gas: soln. of mixture of Re-complex and NEt4OTf inpyridine is stirred overnight; TlCl is filtered off, evapn. of filtrate under vac., extn. with toluene, concn. the volume, recrystn. from CH2Cl2/ether at -40°C, elem. anal.;
DOI:10.1021/om00017a080
upstream raw materials:

[Re(CC6H2(CH3)3)(CO)4(SO3CF3)](1+)*SO3CF3(1-)=[Re(CC6H2(CH3)3)(CO)4(SO3CF3)]SO3CF3

tetraethylammonium chloride

Downstream raw materials:

[Re(CC6H2(CH3)3)(CO)2Cl2(C5H5N)]

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