succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

Base Information

Chemical Name:succinimidyl (1R,2S)-2-azidocyclohexylcarbamate
CAS No.:1427038-68-3
Molecular Formula:C₁₁H₁₅N₅O₄
Molecular Weight:281.271
Hs Code.:

Synonyms:succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

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Chemical Property of succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

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Technology Process of succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

There total 4 articles about succinimidyl (1R,2S)-2-azidocyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-15-7,931-16-8,6850-38-0,6982-39-4,33092-82-9,38898-70-3,74111-21-0,108267-20-5
(1R,2R)-2-aminocyclohexanol

: 1427038-68-3
succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water; 1,4-dioxane / 3 h / 0 °C

2.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 72 h / 55 °C / Inert atmosphere

4.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

4.2: 1 h

With sodium azide; triethylamine; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja401151v

Reference yield:

: 155975-19-2,477584-30-8
(1R,2R)-trans-2-(N-tert-butyloxycarbonyl)amino-1-cyclohexanol

: 1427038-68-3
succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 72 h / 55 °C / Inert atmosphere

3.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

3.2: 1 h

With sodium azide; triethylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja401151v

Reference yield:

: 603128-64-9
(1R,2R)-2-(N-tert-butoxycarbonylamino)-cyclohexan-1-yl methanesulfonate

: 1427038-68-3
succinimidyl (1R,2S)-2-azidocyclohexylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide / N,N-dimethyl-formamide / 72 h / 55 °C / Inert atmosphere

2.1: trifluoroacetic acid / 0.5 h / Inert atmosphere

2.2: 1 h

With sodium azide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ja401151v