4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Base Information

Chemical Name:4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol
CAS No.:909641-62-9
Molecular Formula:C₃₇H₃₈O₂
Molecular Weight:514.708
Hs Code.:

Synonyms:4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Suppliers and Price of 4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

There total 3 articles about 4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid 4-((E)-2-{7-[(E)-2-(4-acetoxy-phenyl)-vinyl]-9,9-dibutyl-9H-fluoren-2-yl}-vinyl)-phenyl ester

: 909641-62-9
4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Guidance literature:: With sodium hydroxide; In ethanol; at 25 ℃; for 2h;
DOI:10.1002/anie.200601246

Reference yield:

: 9,9-bis(n-butyl)-2,7-diiodofluorene

: 909641-62-9
4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(OAc)2; (o-Tol)3P; Et₃N / dimethylformamide / 6 h / 95 °C

2: 0.95 g / NaOH / ethanol / 2 h / 25 °C

With palladium diacetate; sodium hydroxide; triethylamine; tris-(o-tolyl)phosphine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.200601246

Reference yield:

: 2628-16-2
p-acetoxystyrene

: 909641-62-9
4,4'-[(9,9-dibutyl-9H-fluorene-2,7-diyl)di-(1E)-2,1-ethenediyl]bisphenol

Guidance literature:: Multi-step reaction with 2 steps

1: Pd(OAc)2; (o-Tol)3P; Et₃N / dimethylformamide / 6 h / 95 °C

2: 0.95 g / NaOH / ethanol / 2 h / 25 °C

With palladium diacetate; sodium hydroxide; triethylamine; tris-(o-tolyl)phosphine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.200601246