cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

Base Information

Chemical Name:cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate
CAS No.:1300087-62-0
Molecular Formula:C₂₄H₂₅N₅O₂
Molecular Weight:415.495
Hs Code.:

Synonyms:cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

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Chemical Property of cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

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Technology Process of cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

There total 3 articles about cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-amine

: 108-93-0
cyclohexanol

: 1300087-62-0
cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

Guidance literature:: 1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-amine; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 16h; Inert atmosphere;

cyclohexanol; In tetrahydrofuran; for 48h; Inert atmosphere;

Reference yield: 42.0%

: 1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-amine

: 530-62-1
1,1'-carbonyldiimidazole

: 108-93-0
cyclohexanol

: 1300087-62-0
cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

Guidance literature:: 1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-amine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 16h; Inert atmosphere;

cyclohexanol; In tetrahydrofuran; for 48h; Reflux;

Reference yield:

: 146135-18-4
phenylmethyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

: 1300087-62-0
cyclohexyl (1-methyl-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: cyclohexa-1,4-diene / palladium 10% on activated carbon / methanol / 4 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 16 h / Inert atmosphere

2.2: 48 h / Reflux

With cyclohexa-1,4-diene; palladium 10% on activated carbon; In tetrahydrofuran; methanol;