2--2-ethilmalononitrile

Base Information

Chemical Name:2--2-ethilmalononitrile
CAS No.:82992-63-0
Molecular Formula:C₂₁H₂₇N₃O₂
Molecular Weight:353.464
Hs Code.:

2-<t-4-t-butyl-1-(p-nitrophenyl)cyclohexil>-2-ethilmalononitrile

Synonyms:2--2-ethilmalononitrile

Suppliers and Price of 2--2-ethilmalononitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--2-ethilmalononitrile

Chemical Property:

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Technology Process of 2--2-ethilmalononitrile

There total 6 articles about 2--2-ethilmalononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2-ethylmalononitrile sodium salt

: 78928-45-7
c-4-t-butyl-r-1-nitro-1-(p-nitrophenyl)cyclohexane

: 82992-63-0
2--2-ethilmalononitrile

Guidance literature:: In dimethyl sulfoxide; at 55 ℃; for 0.5h; Irradiation;
DOI:10.1016/0040-4020(82)80122-1

Reference yield:

: 4701-98-8
4-tert-butylcyclohexanone oxime

: 82992-63-0
2--2-ethilmalononitrile

Guidance literature:: Multi-step reaction with 5 steps

1: Cl₂

2: O₃

3: NaBH₄ / Pd/C / ethanol / 1 h / Ambient temperature

4: 88 percent / 1.) KOH / 1.) EtOH, 0 deg C, 1h; 2.)DMSO, 24h, rt.

5: 89 percent / dimethylsulfoxide / 0.5 h / 55 °C / Irradiation

With potassium hydroxide; sodium tetrahydroborate; chlorine; ozone; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;
DOI:10.1016/0040-4020(82)80122-1

Reference yield:

: 82992-54-9
c-4-t-butyl-r-1-chloro-1-nitrocyclohexane

: 82992-63-0
2--2-ethilmalononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / Pd/C / ethanol / 1 h / Ambient temperature

2: 88 percent / 1.) KOH / 1.) EtOH, 0 deg C, 1h; 2.)DMSO, 24h, rt.

3: 89 percent / dimethylsulfoxide / 0.5 h / 55 °C / Irradiation

With potassium hydroxide; sodium tetrahydroborate; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;
DOI:10.1016/0040-4020(82)80122-1