N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester
CAS No.:1046453-70-6
Molecular Formula:C₃₂H₃₀NO₆P
Molecular Weight:555.567
Hs Code.:

Synonyms:N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

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Chemical Property of N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

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Technology Process of N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

There total 1 articles about N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 5672-83-3
Z-L-GluOMe

: 60254-10-6
(o-hydroxyphenyl)diphenylphosphine

: 1046453-70-6
N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.carres.2008.04.023

Reference yield: 50.0%

: 1046453-70-6
N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

: 20379-60-6
α-D-Glucopyranosyl azide

: 1046453-75-1
Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-glutamine-O-methyl ester

Guidance literature:: N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester; α-D-Glucopyranosyl azide; In N,N-dimethyl acetamide; at 50 ℃; for 0.833333h; microwave irradiation;

With water; In N,N-dimethyl acetamide; at 50 ℃; for 0.166667h; Further stages.; microwave irradiation;
DOI:10.1016/j.carres.2008.04.023

Reference yield: 40.0%

: 1046453-70-6
N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester

: 20379-60-6
α-D-Glucopyranosyl azide

: 1046453-75-1
Nα-benzyloxycarbonyl-Nγ-α-D-glucopyranosyl-L-glutamine-O-methyl ester

: C₂₀H₂₈N₂O₁₀

Guidance literature:: N-benzyloxycarbonyl-L-glutamic acid 5-(2-diphenylphosphanyl-phenyl)ester 1-methyl ester; α-D-Glucopyranosyl azide; In N,N-dimethyl acetamide; at 40 ℃; for 4h;

With water; In N,N-dimethyl acetamide; at 40 ℃; for 2h; Further stages.;
DOI:10.1016/j.carres.2008.04.023