benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate

Base Information

• Chemical Name: benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate
• CAS No.: 1002347-82-1
• Molecular Formula: C₁₉H₁₉NO₅S
• Molecular Weight: 373.43

Synonyms:benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate

Chemical Property of benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate

Chemical Property:

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Technology Process of benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate

There total 1 articles about benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-(chlorosulfonyl)-2-methylpropanoyl chloride (41138-76-5) + (S)-α-phenylglycine benzyl ester (72028-76-3) → benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate (1002347-82-1)

Guidance literature:

2-(chlorosulfonyl)-2-methylpropanoyl chloride; (S)-α-phenylglycine benzyl ester; In diethyl ether; at -78 ℃; for 0.166667h;

With triethylamine; In diethyl ether; at -78 ℃; Further stages.;

DOI:10.1039/b713899g

Reference yield: 98.0%

benzyl (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetate (1002347-82-1) → (DL)-α-(4,4-dimethyl-1,1-dioxido-3-oxo-1,2-thiazetidin-2-yl)phenylacetic acid

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h; atmospheric pressure;

DOI:10.1039/b713899g

upstream raw materials:

2-(chlorosulfonyl)-2-methylpropanoyl chloride

(S)-α-phenylglycine benzyl ester

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