{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

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Chemical Name:{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone
CAS No.:522614-66-0
Molecular Formula:C₂₉H₇F₁₅N₂O₂
Molecular Weight:700.363
Hs Code.:

{5-[(5-pentafluorobenzoyl-1<i>H</i>-pyrrol-3-yl)-pentafluorophenyl-methyl]-1<i>H</i>-pyrrol-2-yl}-pentafluorophenyl-methanone

Synonyms:{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

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Chemical Property of {5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

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Technology Process of {5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

There total 1 articles about {5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: C₁₅H₉F₅N₂

: pentafluorophenyl-{5-[pentafluorophenyl-(1H-pyrrol-3-yl)-methyl]-1H-pyrrol-2-yl}-methanone

: 522614-68-2
pentafluorophenyl-{4-[pentafluorophenyl-(1H-pyrrol-2-yl)-methyl]-1H-pyrrol-2-yl}-methanone

: 522614-66-0
{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

Guidance literature:: C₁₅H₉F₅N₂; With aluminum (III) chloride; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

pentafluorobenzoylchloride; In dichloromethane; at 20 ℃; for 38h; Inert atmosphere;
DOI:10.1002/anie.201100429

Reference yield:

: 522614-66-0
{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

: 727348-59-6
(5-{[5-(hydroxy-pentafluorophenyl-methyl)-1H-pyrrol-3-yl]-pentafluorophenyl-methyl}-1H-pyrrol-2-yl)-pentafluorophenyl-methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 8h;
DOI:10.1021/ol034227l

Reference yield:

: 522614-66-0
{5-[(5-pentafluorobenzoyl-1H-pyrrol-3-yl)-pentafluorophenyl-methyl]-1H-pyrrol-2-yl}-pentafluorophenyl-methanone

: Ag(III) complex of 5,10,15,20-tetrakis(pentafluorophenyl)-2-aza-21-carbaporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaBH₄ / tetrahydrofuran; methanol / 8 h / 20 °C

2.1: methanesulfonic acid / CH₂Cl₂ / 1.5 h / 20 °C

2.2: 21 percent / DDQ / CH₂Cl₂ / 0.25 h / 20 °C

3.1: 32 percent / AgOCOCF₃; pyridine / CHCl₃ / 168 h / Heating

With pyridine; sodium tetrahydroborate; methanesulfonic acid; silver trifluoroacetate; In tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1021/ol034227l