4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

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Chemical Name:4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester
CAS No.:1027074-75-4
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

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Chemical Property of 4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

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Technology Process of 4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

There total 11 articles about 4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 155128-11-3
(1S,5R,3Z)-3,5-dimethyl-6-(methoxymethoxy)-1-phenylhex-3-en-1-ol

: 62-23-7
4-nitro-benzoic acid

: 1027074-75-4
4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 - 35 ℃; for 20h;
DOI:10.1039/c0ob01084g

Reference yield:

: 100-52-7
benzaldehyde

: 1027074-75-4
4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 3 h / Inert atmosphere; Reflux

1.2: 19 h / 0 - 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / toluene / 20 h / 20 - 35 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triphenylphosphine; diethylazodicarboxylate; In toluene; benzene; 2.1: Mitsunobu reaction;
DOI:10.1039/c0ob01084g

Reference yield:

: C₁₅H₃₀O₂S₂Si

: 1027074-75-4
4-Nitro-benzoic acid (Z)-(1R,5R)-6-methoxymethoxy-3,5-dimethyl-1-phenyl-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 15 h / Reflux

2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 3 h / Inert atmosphere; Reflux

2.2: 19 h / 0 - 20 °C

3.1: triphenylphosphine; diethylazodicarboxylate / toluene / 20 h / 20 - 35 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triphenylphosphine; diethylazodicarboxylate; In toluene; benzene; 3.1: Mitsunobu reaction;
DOI:10.1039/c0ob01084g