benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt

Base Information

• Chemical Name: benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt
• CAS No.: 1248566-70-2
• Molecular Formula: C₂H₂O₄*C₄₂H₄₆N₄O₉
• Molecular Weight: 840.884

Synonyms:benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt

Chemical Property of benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt

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Technology Process of benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt

There total 1 articles about benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C57H56N4O11 (1248566-66-6) + oxalic acid (144-62-7,97993-78-7) → benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt (1248566-70-2)

Guidance literature:

C₅₇H₅₆N₄O₁₁; With morpholine; at 18 ℃; for 0.583333h;

oxalic acid;

DOI:10.1016/j.carres.2010.05.032

Reference yield: 84.0%

benzyl (3R,4R,5S)-4-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate mono-oxalic acid salt (1248566-70-2) → benzyl (3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate (1248566-73-5)

Guidance literature:

With water; lithium hydroxide; In tetrahydrofuran; at 4 ℃; for 17h;

DOI:10.1016/j.carres.2010.05.032

upstream raw materials:

C₅₇H₅₆N₄O₁₁

oxalic acid

Downstream raw materials:

benzyl (3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)oxy-3-benzyloxy-piperidine-5-carboxylate

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