{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

Base Information

Chemical Name:{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}
CAS No.:116148-10-8
Molecular Formula:C₈H₂₀N*C₁₁H₅CrO₅S
Molecular Weight:431.473
Hs Code.:

{(C<sub>2</sub>H<sub>5</sub>)4N}<sup>(1+)</sup>*{Cr(CO)5(S(C<sub>6</sub>H<sub>5</sub>))}<sup>(1-)</sup> = {(C<sub>2</sub>H<sub>5</sub>)4N}{Cr(CO)5(S(C<sub>6</sub>H<sub>5</sub>))}

Synonyms:{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

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Chemical Property of {(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

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Technology Process of {(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

There total 3 articles about {(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.8%

: 3193-72-4
tetraethylammonium phenylthiolate

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 116148-10-8
{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

Guidance literature:: With THF; In tetrahydrofuran; Irradiation (UV/VIS); N2 atmosphere; addn. of soln. of Cr(CO)5*THF in THF (prepd. from photolysis of Cr(CO)6 in THF) to org. compd., stirring (10 min); concn., pptn. on addn. of diethyl ether, recrystn. (THF/diethyl ether/hexane 1:1:1);

Reference yield:

: 116148-15-3
{Et4N}2{Cr2(CO)8(μ-SPh)2}

: 116148-10-8
{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

Guidance literature:: With CO; In acetonitrile; N2 atmosphere; soln. of carbonyl-compd. in MeCN, evacuation, filling with CO (1 atm), stirring (10 min); removal of MeCN (vac.), recrystn. (THF/hexane); IR monitoring;

Reference yield:

: 3193-72-4
tetraethylammonium phenylthiolate

: 116148-10-8
{(C₂H₅)4N}⁽¹⁺⁾*{Cr(CO)5(S(C₆H₅))}^(1-) = {(C₂H₅)4N}{Cr(CO)5(S(C₆H₅))}

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: CO / acetonitrile

With CO; In tetrahydrofuran; acetonitrile;