3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

Base Information

Chemical Name:3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide
CAS No.:292072-99-2
Molecular Formula:C₃₀H₄₀N₄O₆
Molecular Weight:552.671
Hs Code.:

Synonyms:3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

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Chemical Property of 3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

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Technology Process of 3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

There total 5 articles about 3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4244-84-2
ethyl β-alaninate hydrochloride

: 292072-99-2
3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / toluene / 24 h / 20 °C

2: 3.34 g / methanol / 48 h / 20 °C

With triethylamine; In methanol; toluene; 1: Condensation / 2: Addition;
DOI:10.1016/S0968-0896(00)00066-3

Reference yield:

: 100-52-7
benzaldehyde

: 292072-99-2
3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / toluene / 24 h / 20 °C

2: 3.34 g / methanol / 48 h / 20 °C

With triethylamine; In methanol; toluene; 1: Condensation / 2: Addition;
DOI:10.1016/S0968-0896(00)00066-3

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 292072-99-2
3-[(2-ethoxycarbonylethyl)-thyminacetyl-amino]-phenyl-acetic acid-(4-tert-butyl-cyclohexen-1-yl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / aq. H₂SO₄ / toluene / 12 h / Heating; Dean-Stark-conditions

2: 80 percent / phosgene; NEt₃ / CH₂Cl₂ / 1 h / 0 °C

3: 3.34 g / methanol / 48 h / 20 °C

With phosgene; sulfuric acid; triethylamine; In methanol; dichloromethane; toluene; 1: Condensation / 2: Dehydration / 3: Addition;
DOI:10.1016/S0968-0896(00)00066-3