N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

Base Information

Chemical Name:N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline
CAS No.:205263-05-4
Molecular Formula:C₂₃H₂₄ClNO₃
Molecular Weight:397.901
Hs Code.:

Synonyms:N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

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Chemical Property of N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

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Technology Process of N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

There total 3 articles about N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 205263-05-4
N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / zinc chloride / ethanol / 1 h / Heating

2: 52 percent / p-toluenesulfonic acid monohydrate, 4 Angstroem molecular sieves / benzene / 20 h / Heating

3: 93 percent / sodium borohydride / methanol / 2 h / Ambient temperature

4: 44 percent / pyridine / 0 deg C, 30 min then r.t., 1 h

With pyridine; sodium tetrahydroborate; 4 A molecular sieve; toluene-4-sulfonic acid; zinc(II) chloride; In methanol; ethanol; benzene;
DOI:10.3987/COM-97-8022

Reference yield:

: 205262-91-5
3-acetyl-2,4,5-trimethylfuran

: 205263-05-4
N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / p-toluenesulfonic acid monohydrate, 4 Angstroem molecular sieves / benzene / 20 h / Heating

2: 93 percent / sodium borohydride / methanol / 2 h / Ambient temperature

3: 44 percent / pyridine / 0 deg C, 30 min then r.t., 1 h

With pyridine; sodium tetrahydroborate; 4 A molecular sieve; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.3987/COM-97-8022

Reference yield:

: 205262-94-8
4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethylidene]aniline

: 205263-05-4
N-benzyloxycarbonyl-4-chloro-N-[1-(2',4',5'-trimethylfur-3'-yl)ethyl]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / sodium borohydride / methanol / 2 h / Ambient temperature

2: 44 percent / pyridine / 0 deg C, 30 min then r.t., 1 h

With pyridine; sodium tetrahydroborate; In methanol;
DOI:10.3987/COM-97-8022