4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester

Base Information

• Chemical Name: 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester
• CAS No.: 1605324-70-6
• Molecular Formula: C₁₄H₁₉NO₄
• Molecular Weight: 267.293

Synonyms:4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester

Chemical Property of 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester

There total 2 articles about 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tert-butyldicarbonate (34619-03-9) + 4-cyanobenzoic acid methyl ester (1129-35-7) → 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester (1605324-70-6)

Guidance literature:

With palladium 10% on activated carbon; deuterium; In ethanol-d6; at 20 ℃; for 20h; under 2327.23 Torr; Reagent/catalyst; Solvent;

Reference yield: 95.0%

4-cyanobenzoic acid methyl ester (1129-35-7) + di-tert-butyl dicarbonate (24424-99-5) → 4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester (1605324-70-6)

Guidance literature:

With deuterium; ethyl [2]alcohol; palladium 10% on activated carbon; at 20 ℃; for 20h; under 2327.23 Torr; Reagent/catalyst;

DOI:10.1016/j.ejmech.2021.113666

Reference yield: 92.0%

4-(tert-butoxycarbonylamino-dideutero-methyl)-benzoic acid methyl ester (1605324-70-6) → 4-(amino-dideutero-methyl)-benzoic acid methyl ester hydrochloride (1605324-71-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 2h; Inert atmosphere;

DOI:10.1016/j.ejmech.2021.113666

upstream raw materials:

tert-butyldicarbonate

4-cyanobenzoic acid methyl ester

di-tert-butyl dicarbonate

Downstream raw materials:

4-(amino-dideutero-methyl)-benzoic acid methyl ester hydrochloride

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