C₃₁H₃₆Cl₃NO₁₀

Base Information

Chemical Name:C₃₁H₃₆Cl₃NO₁₀
CAS No.:1577227-95-2
Molecular Formula:C₃₁H₃₆Cl₃NO₁₀
Molecular Weight:688.987
Hs Code.:

C<sub>31</sub>H<sub>36</sub>Cl<sub>3</sub>NO<sub>10</sub>

Synonyms:C₃₁H₃₆Cl₃NO₁₀

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Chemical Property of C₃₁H₃₆Cl₃NO₁₀

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Technology Process of C₃₁H₃₆Cl₃NO₁₀

There total 5 articles about C₃₁H₃₆Cl₃NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₆O₁₀

: 545-06-2
trichloroacetonitrile

: 1577227-95-2
C₃₁H₃₆Cl₃NO₁₀

Guidance literature:: With sodium hydride; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577227-58-7
dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

: 1577227-95-2
C₃₁H₃₆Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 1 h / -78 °C / Molecular sieve; Inert atmosphere

1.3: Molecular sieve; Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C / Inert atmosphere

3.1: pyridine; dmap / 4 h / 0 - 20 °C / Inert atmosphere

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

5.1: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c3ob42312c

Reference yield:

: 1577228-10-4
dimethylthexylsilyl 3,4-O-benzyl-β-D-glucopyranoside

: 1577227-95-2
C₃₁H₃₆Cl₃NO₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C / Inert atmosphere

2: pyridine; dmap / 4 h / 0 - 20 °C / Inert atmosphere

3: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / Inert atmosphere

4: sodium hydride / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

With pyridine; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; sodium hydride; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c3ob42312c