2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of

Base Information

• Chemical Name: 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of
• CAS No.: 910449-96-6
• Molecular Formula: C₃₀H₄₁N₅O₈
• Molecular Weight: 599.684

Synonyms:2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of

Chemical Property of 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of

Chemical Property:

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Technology Process of 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of

There total 2 articles about 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-nitrophenyl)-2-(3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1(14),11(15),12-trien-3-yl)butyric acid, methyl ester of (596121-70-9) + ethyl bromoacetate (105-36-2) → 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1(14),11(15),12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of (910449-96-6)

Guidance literature:

With potassium carbonate; In di-isopropyl ether; acetonitrile; for 24h; Reflux;

Reference yield:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(14),11(15),12-triene (78668-34-5) + d,l-2-bromo-4-(4-nitrophenyl)butanoic acid methyl ester (130707-80-1) → 2-(6,9-bis(ethoxycarbonylmethyl)-3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1(14),11(15),12-trien-3-yl)-4-(4-nitrophenyl)butyric acid, methyl ester of (910449-96-6)

Guidance literature:

Multi-step reaction with 2 steps

1: Amberlite_.(R). IRA₄₅₈ / acetonitrile / 72 h / 25 °C

2: potassium carbonate / di-isopropyl ether; acetonitrile / 24 h / Reflux

With potassium carbonate; In di-isopropyl ether; acetonitrile;

upstream raw materials:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-triene

d,l-2-bromo-4-(4-nitrophenyl)butanoic acid methyl ester

4-(4-nitrophenyl)-2-(3,6,9,15-tetraazabicyclo-[9.3.1]pentadeca-1⁽¹⁴⁾,11⁽¹⁵⁾,12-trien-3-yl)butyric acid, methyl ester of

ethyl bromoacetate

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