[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

Base Information

Chemical Name:[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone
CAS No.:1320259-60-6
Molecular Formula:C₂₂H₂₈O₉
Molecular Weight:436.459
Hs Code.:

Synonyms:[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

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Chemical Property of [2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

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Technology Process of [2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

There total 5 articles about [2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1320259-58-2
[2,6-bis(methoxymethoxy)-4-methylphenyl][4-methoxy-2-(methoxymethoxy)-6-[(phenylmethoxy)methyl]phenyl]-methanone

: 1320259-60-6
[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ol201561w

Reference yield:

: 1320259-54-8
4-methoxy-2-methoxymethoxy6-[(phenylmethoxy)methyl]-benzaldehyde

: 1320259-60-6
[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 25 °C / Inert atmosphere

1.2: 4 h / 0 - 25 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 3.5 h / 25 °C / Inert atmosphere

3.1: 20 % Pd(OH)2/C; hydrogen / methanol / 2 h / 20 °C

With n-butyllithium; 20 % Pd(OH)2/C; hydrogen; Dess-Martin periodane; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol201561w

Reference yield:

: 1320259-56-0
2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

: 1320259-60-6
[2,6-bis(methoxymethoxy)-4-methylphenyl][6-hydroxymethyl-4-methoxy-2-(methoxymethoxy)phenyl]-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 3.5 h / 25 °C / Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / methanol / 2 h / 20 °C

With 20 % Pd(OH)2/C; hydrogen; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1021/ol201561w