2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

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Chemical Name:2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol
CAS No.:1320259-56-0
Molecular Formula:C₂₉H₃₆O₉
Molecular Weight:528.599
Hs Code.:

Synonyms:2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

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Chemical Property of 2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

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Technology Process of 2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

There total 3 articles about 2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1320259-54-8
4-methoxy-2-methoxymethoxy6-[(phenylmethoxy)methyl]-benzaldehyde

: 82265-37-0
1,3-bis(methoxymethoxy)-5-methylbenzene

: 1320259-56-0
2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

Guidance literature:: 1,3-bis(methoxymethoxy)-5-methylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 25 ℃; for 0.333333h; Inert atmosphere;

4-methoxy-2-methoxymethoxy6-[(phenylmethoxy)methyl]-benzaldehyde; In tetrahydrofuran; hexane; at 0 - 25 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol201561w

Reference yield:

: 1320259-48-0
2-hydroxy-4-methoxy-6-[(phenylmethoxy)methyl]-benzaldehyde

: 1320259-56-0
2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 25 °C / Inert atmosphere

2.2: 4 h / 0 - 25 °C / Inert atmosphere

With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol201561w

Reference yield:

: 261958-55-8
2,4-dihydroxy-6-[(phenylmethoxy)methyl]-benzaldehyde

: 1320259-56-0
2,6-bis(methoxymethoxy)-α-[4-methoxy-2-methoxymethoxy-6-[(phenylmethoxy)-methyl]]-4-methyl-benzenemethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 4 h / 25 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 25 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 25 °C / Inert atmosphere

3.2: 4 h / 0 - 25 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; acetone;
DOI:10.1021/ol201561w