C₂₃H₁₉F₄NO₃

Base Information

Chemical Name:C₂₃H₁₉F₄NO₃
CAS No.:1427407-22-4
Molecular Formula:C₂₃H₁₉F₄NO₃
Molecular Weight:433.402
Hs Code.:

C<sub>23</sub>H<sub>19</sub>F<sub>4</sub>NO<sub>3</sub>

Synonyms:C₂₃H₁₉F₄NO₃

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Chemical Property of C₂₃H₁₉F₄NO₃

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Technology Process of C₂₃H₁₉F₄NO₃

There total 6 articles about C₂₃H₁₉F₄NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1427407-21-3
2,4-difluoro-3-[[3-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol

: 105-36-2
ethyl bromoacetate

: 1427407-22-4
C₂₃H₁₉F₄NO₃

Guidance literature:: 2,4-difluoro-3-[[3-fluoro-5-(3-fluorophenyl)phenyl]methylamino]phenol; With caesium carbonate; In acetone; at 20 ℃; for 0.5h;

ethyl bromoacetate; In acetone; at 20 ℃; for 1h;

Reference yield:

: 176548-70-2
3-bromo-5-fluorobenzoic acid

: 1427407-22-4
C₂₃H₁₉F₄NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; ethanol; N,N-dimethyl-formamide / 100 °C / Inert atmosphere

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

3.1: sodium hydrogencarbonate / tetrahydrofuran / 1 h / 0 - 20 °C

4.1: borane-THF / tetrahydrofuran / 0 - 60 °C

5.1: caesium carbonate / acetone / 0.5 h / 20 °C

5.2: 1 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; borane-THF; oxalyl dichloride; sodium hydrogencarbonate; sodium carbonate; caesium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1214352-92-7
C₁₃H₇ClF₂O

: 1427407-22-4
C₂₃H₁₉F₄NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: borane-THF / tetrahydrofuran / 0 - 60 °C

3.1: caesium carbonate / acetone / 0.5 h / 20 °C

3.2: 1 h / 20 °C

With borane-THF; sodium hydrogencarbonate; caesium carbonate; In tetrahydrofuran; acetone;