1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

Base Information

Chemical Name:1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone
CAS No.:1345823-35-9
Molecular Formula:C₁₉H₁₇Cl₂N₃O
Molecular Weight:374.269
Hs Code.:

Synonyms:1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

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Chemical Property of 1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

Chemical Property:

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Technology Process of 1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

There total 4 articles about 1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1345823-24-6
1-(2,4-dichlorophenyl)-4-(trimethylsilyl)but-3-yn-2-one

: 222716-36-1
1-(azidomethyl)-3,5-dimethylbenzene

: 1345823-35-9
1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

Guidance literature:: With sodium L-ascorbate; copper dichloride; In water; acetonitrile; at 20 ℃; Reflux;
DOI:10.1016/j.ejmech.2011.09.013

Reference yield:

: 19719-28-9
2,4-dichlorophenylacetic acid

: 1345823-35-9
1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / dichloromethane / Reflux

2: aluminum (III) chloride / dichloromethane / 0 °C

3: sodium L-ascorbate; copper dichloride / water; acetonitrile / 20 °C / Reflux

With aluminum (III) chloride; thionyl chloride; sodium L-ascorbate; copper dichloride; In dichloromethane; water; acetonitrile; 3: Huisgen cycloaddition;
DOI:10.1016/j.ejmech.2011.09.013

Reference yield:

: 53056-20-5
2,4-dichlorophenylacetyl chloride

: 1345823-35-9
1-(1-(3,5-dimethylbenzyl)-1H-1,2,3-triazol-4-yl)-2-(2,4-dichlorophenyl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0 °C

2: sodium L-ascorbate; copper dichloride / water; acetonitrile / 20 °C / Reflux

With aluminum (III) chloride; sodium L-ascorbate; copper dichloride; In dichloromethane; water; acetonitrile; 2: Huisgen cycloaddition;
DOI:10.1016/j.ejmech.2011.09.013