anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid

Base Information

• Chemical Name: anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid
• CAS No.: 81268-09-9
• Molecular Formula: C₂₇H₂₂N₃O₃P
• Molecular Weight: 467.464

Synonyms:anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid

Chemical Property of anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid

Chemical Property:

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Technology Process of anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid

There total 3 articles about anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarbonsaeure-phenylimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + cyclohepta-2,4,6-trien-1-yldiphenylphosphine oxide (81268-06-6) → anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.02,4>non-8-en-6,7-dicarbonsaeure-phenylimid (81268-09-9)

Guidance literature:

In diethyl ether; acetone; at 0 ℃;

Reference yield:

diphenylphosphinous acid methyl ester (4020-99-9) → anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.02,4>non-8-en-6,7-dicarbonsaeure-phenylimid (81268-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / acetonitrile / 0.75 h / Heating

2: 90 percent / acetone; diethyl ether / 0 °C

In diethyl ether; acetone; acetonitrile;

Reference yield:

tropylium bromide → anti-3-Diphenylphosphoryl-6,7-diaza-exo-tricyclo<3.2.2.02,4>non-8-en-6,7-dicarbonsaeure-phenylimid (81268-09-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / acetonitrile / 0.75 h / Heating

2: 90 percent / acetone; diethyl ether / 0 °C

In diethyl ether; acetone; acetonitrile;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

cyclohepta-2,4,6-trien-1-yldiphenylphosphine oxide

diphenylphosphinous acid methyl ester

Downstream raw materials:

anti-9-diphenylphosphoryl-5-methyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

anti-9-diphenylphosphoryl-5,5-dimethyl-3,4,11,12-tetraza-exo,endo-tetracyclo<5.3.2.0^2,6.0^8,10>dodec-3-ene-11,12-dicarboxylic acid phenylimide

anti-3-diphenylphosphoryl-7,7-dimethyl-9,10-diaza-endo,exo-tetracyclo<3.3.2.0^2,4.0^6,8>decane-9,10-dicarboxylic acid phenylimide

anti-3-diphenylphosphoryl-anti-7-methyl-9,10-diaza-endo,exo-tetracyclo<3.3.2.0^2,4.0^6,8>decane-9,10-dicarboxylic acid phenylimide

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