{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

Base Information

Chemical Name:{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾
CAS No.:97879-05-5
Molecular Formula:C₂₂H₁₅CrNO₅
Molecular Weight:425.361
Hs Code.:

{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium<sup>(0)</sup>

Synonyms:{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

Suppliers and Price of {3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

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Technology Process of {3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

There total 2 articles about {3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 15975-93-6
pentacarbonyl((methyl)((tetramethylammonio)oxy)carbene)chromium⁽⁰⁾

: 622-29-7
N-Benzylidenemethylamine

: 97879-05-5
{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

Guidance literature:: With toluene-4-sulfonyl chloride; In dichloromethane; Chromium compound is dissolved at room temp. and a soln. of TsCl is added dropwise with stirring (N2). After 10 min ArCH=NMe is added and the mixture is stirred at room temp. for 8 h.; removal of solvent, chromy. on silica (hexane/Et2O); elem. anal.;

Reference yield: 9.0%

: 15975-93-6
pentacarbonyl((methyl)((tetramethylammonio)oxy)carbene)chromium⁽⁰⁾

: 622-29-7
N-Benzylidenemethylamine

: 88034-35-9
pentacarbonyl{1-(1-methoxy-3(E)-phenyl-2-propenylidene)}chromium⁽⁰⁾

: 97879-05-5
{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

Guidance literature:: With toluene-4-sulfonyl chloride; methanol; In dichloromethane; Chromium compound is dissolved at room temp. and a soln. of TsCl is added dropwise with stirring (N2). After 5 min ArCH=NMe is added dropwise and stirring is continued for 10 min. MeOH is added and the mixture is stirred for 3.5 h.; removal of solvent, chromy. on silica (hexane/Et2O);

Reference yield: 97.0%

: 97879-05-5
{3(E)-benzylidene-1-methyl-4-phenylazetidinylidene}-pentacarbonylchromium⁽⁰⁾

: 536-80-1
iodosylbenzene

: 97879-03-3
(E)-3-benzylidene-1-methyl-4-phenyl-2-azetidinone

Guidance literature:: In dichloromethane; A soln. of chromium compound is added to PhIO and stirred for 4 days.; evapn. of solvent, chromy.; elem. anal., mp, IR, NMR, UV, MS;