Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)

Base Information

Chemical Name:Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)
CAS No.:85661-24-1
Molecular Formula:C₆H₆N₂O₃
Molecular Weight:154.125
Hs Code.:2933990090
Mol file:85661-24-1.mol

Synonyms:Pyrazinecarboxylicacid, methyl ester, 1-oxide (9CI); 2-Methoxycarbonylpyrazine 1-oxide

Suppliers and Price of Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)

Chemical Property:

PSA：64.65000
LogP:0.29670

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)

There total 1 articles about Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 6164-79-0
methyl pyrazine-2-carboxylate

: 85661-24-1
2-(methoxycarbonyl)pyrazine 1-oxide

: 770-00-3
methylester of pyrazinecarboxylic acid 4-oxide

Guidance literature:: With potassium peroxomonosulphate; In sulfuric acid; for 24h; Ambient temperature;

Reference yield:

: 85661-24-1
2-(methoxycarbonyl)pyrazine 1-oxide

: 1197237-46-9
1-(6-chloropyrazin-2-yl)ethanone

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 85 °C

2: sodium tetrahydroborate / water / 0 - 20 °C

3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C

4: tetrahydrofuran / 1 h / -5 - 20 °C

5: Dess-Martin periodane / dichloromethane / 3 h / 20 °C

With sodium tetrahydroborate; thionyl chloride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 85661-24-1
2-(methoxycarbonyl)pyrazine 1-oxide

: 1240602-95-2
(6-chloropyrazin-2-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 85 °C

2: sodium tetrahydroborate / water / 0 - 20 °C

With sodium tetrahydroborate; thionyl chloride; In water;