Technology Process of Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI)
There total 1 articles about Pyrazinecarboxylic acid, methyl ester, 1-oxide (9CI) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium peroxomonosulphate;
In
sulfuric acid;
for 24h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 85 °C
2: sodium tetrahydroborate / water / 0 - 20 °C
3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
4: tetrahydrofuran / 1 h / -5 - 20 °C
5: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
With
sodium tetrahydroborate; thionyl chloride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / 85 °C
2: sodium tetrahydroborate / water / 0 - 20 °C
With
sodium tetrahydroborate; thionyl chloride;
In
water;