N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Base Information

Chemical Name:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester
CAS No.:395647-19-5
Molecular Formula:C₂₆H₃₄N₄O₅
Molecular Weight:482.58
Hs Code.:

Synonyms:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Suppliers and Price of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

There total 4 articles about N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 395647-12-8
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}valine methyl ester

: 395647-19-5
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Guidance literature:: With dmap; In acetonitrile;
DOI:10.1016/S0040-4039(01)01350-8

Reference yield:

: 20691-84-3
m-methyl red

: 395647-19-5
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / DCC; HOBt / dimethylformamide

2: 85 percent / DMAP / acetonitrile / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j

Reference yield:

: 6306-52-1
L-valine methylester hydrochloride

: 395647-19-5
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylvaline methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / DCC; HOBt / dimethylformamide

2: 85 percent / DMAP / acetonitrile / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j