phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

Base Information

Chemical Name:phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside
CAS No.:132351-74-7
Molecular Formula:C₁₉H₃₀O₃Si
Molecular Weight:334.531
Hs Code.:

Synonyms:phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

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Chemical Property of phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

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Technology Process of phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

There total 9 articles about phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 76404-30-3
Benzyl-2,3,6-tridesoxy-α-L-erythro-hex-2-enopyranosid

: 132351-74-7
phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane;
DOI:10.1021/jo951560x

Reference yield:

: 76404-29-0
phenylmethyl 4-O-acetyl-2,3,6-trideoxy-α-L-erythro-hex-2-enopyranoside

: 132351-74-7
phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / methanol

2: 91 percent / imidazole / CH₂Cl₂

With 1H-imidazole; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo951560x

Reference yield:

: 34819-86-8
3,4-di-O-acetyl-6-deoxy-L-glucal

: 132351-74-7
phenylmethyl 2,3,6-trideoxy-4-O-<(1,1-dimethylethyl)dimethylsilyl>-α-L-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: BF₃*Et₂O / CH₂Cl₂

2: NaOMe / methanol

3: 91 percent / imidazole / CH₂Cl₂

With 1H-imidazole; boron trifluoride diethyl etherate; sodium methylate; In methanol; dichloromethane;
DOI:10.1021/jo951560x