[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

Base Information

Chemical Name:[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone
CAS No.:248253-34-1
Molecular Formula:C₂₆H₂₈NO₅P
Molecular Weight:465.486
Hs Code.:

Synonyms:[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

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Chemical Property of [2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

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Technology Process of [2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

There total 3 articles about [2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 144630-67-1
2-(diphenylphosphoryl)pyrrolidine

: 248253-34-1
[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: With triethylamine; In toluene;
DOI:10.1002/(SICI)1099-0690(199909)1999:9<2345::AID-EJOC2345>3.0.CO;2-P

Reference yield: 78.0%

: 144630-67-1
2-(diphenylphosphoryl)pyrrolidine

: 118-41-2
Eudesmic acid

: 248253-34-1
[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0968-0896(00)00130-9

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 248253-34-1
[2-(diphenyl-phosphinoyl)-pyrrolidin-1-yl]-(3,4,5-trimethoxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / toluene / Heating

2: 78 percent / DCC; DMAP; Et₃N / CH₂Cl₂

With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; toluene; 1: Substitution / 2: Acylation;
DOI:10.1016/S0968-0896(00)00130-9