2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

Base Information

Chemical Name:2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione
CAS No.:1325219-62-2
Molecular Formula:C₅₄H₆₆N₂O₂
Molecular Weight:775.13
Hs Code.:

Synonyms:2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

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Chemical Property of 2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

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Technology Process of 2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

There total 5 articles about 2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1325219-56-4
N-butyl-N-(2-ethylhexyl)-4-ethynylbenzeneamine

: 78507-46-7
2,6-diiodoanthracene-9,10-dione

: 1325219-62-2
2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 80 ℃; Inert atmosphere;
DOI:10.1002/pola.24806

Reference yield:

: 1325219-55-3
4-(4-(butyl(2-ethylhexyl)amino)phenyl)-2-methylbut-3-yn-2-ol

: 1325219-62-2
2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / toluene / Inert atmosphere; Reflux

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; potassium hydroxide; In tetrahydrofuran; toluene; 2: Sonogashira coupling;
DOI:10.1002/pola.24806

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1325219-62-2
2,6-bis((4-(butyl(2-ethylhexyl)amino)phenyl)ethynyl)anthracene-9,10-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammomium bromide; sodium carbonate; potassium iodide / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

1.2: 72 h / 110 °C / Inert atmosphere

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 40 °C / Inert atmosphere

3.1: potassium hydroxide / toluene / Inert atmosphere; Reflux

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 80 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutylammomium bromide; sodium carbonate; triethylamine; potassium iodide; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 2.1: Sonogashira coupling / 4.1: Sonogashira coupling;
DOI:10.1002/pola.24806