di-tert-butyl cyclopropane-1,1-dicarboxylate

Base Information

Chemical Name:di-tert-butyl cyclopropane-1,1-dicarboxylate
CAS No.:18721-68-1
Molecular Formula:C₁₃H₂₂O₄
Molecular Weight:242.315
Hs Code.:

Synonyms:di-tert-butyl cyclopropane-1,1-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl cyclopropane-1,1-dicarboxylate

Chemical Property:

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Technology Process of di-tert-butyl cyclopropane-1,1-dicarboxylate

There total 1 articles about di-tert-butyl cyclopropane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18719-42-1
diethyl 2-chloroethylmalonate

: 865-47-4
potassium tert-butylate

: 18721-68-1
di-tert-butyl cyclopropane-1,1-dicarboxylate

Guidance literature:: In tert-butyl alcohol;
DOI:10.1039/j29680000067

Reference yield: 47.0%

: 1829-28-3
ethyl 2-iodobenzoate

: 18721-68-1
di-tert-butyl cyclopropane-1,1-dicarboxylate

: di-tert-butyl 2-(2-(ethoxycarbonyl)phenethyl)malonate

Guidance literature:: ethyl 2-iodobenzoate; With TurboGrignard; In tetrahydrofuran; 2-methyltetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere; Sealed tube;

di-tert-butyl cyclopropane-1,1-dicarboxylate; With 1,3-dimethyl-2-imidazolidinone; copper(I) iodide dimethyl sulfide complex; In tetrahydrofuran; 2-methyltetrahydrofuran; at -78 - 23 ℃; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.8b00754

Reference yield:

: 18721-68-1
di-tert-butyl cyclopropane-1,1-dicarboxylate

: 1137-96-8,26505-49-7,201024-81-9
N-(benzylidene)aniline N-oxide

: (+)-2,3-diphenyl-[1,2]oxazinane-4,4-dicarboxylic acid di-tert-butyl ester

: (-)-diphenyl-[1,2]oxazinane-4,4-dicarboxylic acid di-tert-butyl ester

Guidance literature:: With 4 A molecular sieve; chiral (S,S)-bisoxazoline derivative; nickel(II) perchlorate; In dichloromethane; at 20 ℃; for 60h; Title compound not separated from byproducts;
DOI:10.1021/ja0421497