[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

Base Information

Chemical Name:[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester
CAS No.:88352-83-4
Molecular Formula:C₂₇H₃₄ClNO₄
Molecular Weight:472.024
Hs Code.:

Synonyms:[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

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Chemical Property of [2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

Chemical Property:

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Technology Process of [2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

There total 6 articles about [2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 112-53-8
1-dodecyl alcohol

: 88352-70-9
TA-1801A

: 88352-83-4
[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm00401a021

Reference yield:

: 88352-86-7
(furan-2-ylcarbonyl)methylamine hydrochloride

: 88352-83-4
[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / NaHCO₃ / H₂O; ethyl acetate / Ambient temperature

2: 70 percent / NaH / paraffin; dimethylformamide / 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min

3: 86 percent / phosphoryl chloride / dimethylformamide / 8 h / Ambient temperature

4: 91 percent / KOH / methanol; H₂O / 8 h / 50 °C

5: 47 percent / CMPI, Et₃N / tetrahydrofuran / Ambient temperature

With potassium hydroxide; sodium hydride; sodium hydrogencarbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide; paraffin;
DOI:10.1021/jm00401a021

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 88352-83-4
[2-(4-Chloro-phenyl)-5-furan-2-yl-oxazol-4-yl]-acetic acid dodecyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / NaHCO₃ / H₂O; ethyl acetate / Ambient temperature

2: 70 percent / NaH / paraffin; dimethylformamide / 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min

3: 86 percent / phosphoryl chloride / dimethylformamide / 8 h / Ambient temperature

4: 91 percent / KOH / methanol; H₂O / 8 h / 50 °C

5: 47 percent / CMPI, Et₃N / tetrahydrofuran / Ambient temperature

With potassium hydroxide; sodium hydride; sodium hydrogencarbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide; paraffin;
DOI:10.1021/jm00401a021