1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

Base Information

Chemical Name:1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene
CAS No.:138962-69-3
Molecular Formula:C₁₆H₁₃N₃S₂
Molecular Weight:311.431
Hs Code.:

Synonyms:1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

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Technology Process of 1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

There total 2 articles about 1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 138962-90-0
4-Phenyl-2,4-dihydro-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene-1-thione

: 74-88-4
methyl iodide

: 138962-69-3
1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

Guidance literature:: With potassium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1016/0223-5234(91)90011-B

Reference yield:

: 130336-92-4
C₂₁H₁₈N₄S₂

: 138962-69-3
1-Methylsulfanyl-4-phenyl-4H-5-thia-2,3,9b-triaza-cyclopenta[a]naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / dimethylformamide / 2 h / Heating

2: 89 percent / TBAB, KOH / tetrahydrofuran / 1 h / Ambient temperature

With potassium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(91)90011-B