(2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone

Base Information

• Chemical Name: (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone
• CAS No.: 1454287-74-1
• Molecular Formula: C₂₁H₁₄ClNOS
• Molecular Weight: 363.867
• Mol file: 1454287-74-1.mol

Synonyms:(2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone

Chemical Property of (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone

There total 2 articles about (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

6-chloro-2-(2-methylphenyl)-1,3-benzothiazole (1242307-44-3) + benzyl alcohol (100-51-6,185532-71-2) → (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone (1454287-74-1)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; p-benzoquinone; In chlorobenzene; at 110 ℃; for 2h; Sealed tube;

DOI:10.1016/j.tet.2013.08.005

Reference yield: 67.0%

6-chloro-2-(2-methylphenyl)-1,3-benzothiazole (1242307-44-3) + benzaldehyde (100-52-7) → (2-(6-chlorobenzo[d]thiazol-2-yl)-3-methylphenyl)(phenyl)methanone (1454287-74-1)

Guidance literature:

With tert.-butylhydroperoxide; palladium diacetate; acetic acid; at 120 ℃; for 2h; regioselective reaction;

DOI:10.3184/174751913X13639769724276

upstream raw materials:

6-chloro-2-(2-methylphenyl)-1,3-benzothiazole

benzyl alcohol

benzaldehyde