(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

Base Information

Chemical Name:(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester
CAS No.:279240-37-8
Molecular Formula:C₂₇H₃₀Cl₂N₂O₅
Molecular Weight:533.452
Hs Code.:

Synonyms:(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

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Technology Process of (1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

There total 1 articles about (1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 279240-36-7
(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-amino-L-phenylalanine methyl ester

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: 279240-37-8
(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 0.25h;

Reference yield:

: 279240-37-8
(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

: 279240-38-9
[1S-(1α,3α)]-4-[(2,6-dichlorobenzoyl)amino]-N-[[3-(1-hydroxyethyl)-2,2-dimethylcyclobutyl]acetyl]-L-phenylalanine methyl ester

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; at -20 - 0 ℃; for 5h;

Reference yield:

: 279240-37-8
(1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester

: (1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl)amino]-L-phenylalanine

Guidance literature:: (1S-cis)-N-[(3-acetyl-2,2-dimethylcyclobutyl)acetyl]-4-[(2,6-dichlorobenzoyl) amino]-L-phenylalanine methyl ester; With lithium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;