(1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine

Base Information

• Chemical Name: (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine
• CAS No.: 1383611-02-6
• Molecular Formula: C₃₂H₄₂N₂S₂
• Molecular Weight: 518.831
• Mol file: 1383611-02-6.mol

Synonyms:(1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine

Chemical Property of (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine

There total 3 articles about (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(1R,2R)-1,2-diaminocyclohexane (20439-47-8) + 2-(cyclohexylsulfanyl)benzaldehyde (503065-08-5) → (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine (1383611-02-6)

Guidance literature:

In ethanol; at 80 ℃;

DOI:10.1002/anie.201304844

Reference yield:

Cyclohexanethiol (1569-69-3) + 2-nitro-benzaldehyde (552-89-6) → (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine (1383611-02-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 - 80 °C

2: ethanol / 80 °C

With potassium carbonate; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/anie.201304844

Reference yield:

→ (1R,2R)-N,N'-bis(2-(cyclohexylthio)benzylidene)-1,2-cyclohexanediamine (1383611-02-6)

Guidance literature:

upstream raw materials:

(1R,2R)-1,2-diaminocyclohexane

2-(cyclohexylsulfanyl)benzaldehyde

Cyclohexanethiol

2-nitro-benzaldehyde

Downstream raw materials:

(1R,2R)-N,N'-bis(2-(cyclohexylthio)benzyl)-1,2-cyclohexanediamine