phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside
CAS No.:1447811-14-4
Molecular Formula:C₂₃H₃₆F₃NO₅SSi
Molecular Weight:523.689
Hs Code.:

Synonyms:phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

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Technology Process of phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

There total 1 articles about phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1447811-13-3
phenyl 2-amino-2-deoxy-1-thio-6-O-(triisopropylsilyl)-β-D-glucopyranoside

: 407-25-0
trifluoroacetic anhydride

: 1447811-14-4
phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.05.036

Reference yield: 83.0%

: 1447811-14-4
phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 1447811-15-5
phenyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.05.036

Reference yield:

: 1447811-14-4
phenyl 2-deoxy-1-thio-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

: 1447811-16-6
1-O-(2-benzyloxyethyl)-2-deoxy-3,4-di-O-benzoyl-2-trifluoroacetylamino-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 20 h / 20 °C / Inert atmosphere

2: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 20 °C / Molecular sieve; Inert atmosphere

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2013.05.036