Technology Process of C36H56O3
There total 3 articles about C36H56O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
nickel(II) nitrate hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen; triethylamine; copper dichloride;
In
methanol;
at 120 ℃;
for 1.5h;
under 760.051 Torr;
Inert atmosphere;
DOI:10.1039/c3gc40872h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 60 °C / Inert atmosphere
3: triethylamine; copper dichloride; nickel(II) nitrate hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen / methanol / 1.5 h / 120 °C / 760.05 Torr / Inert atmosphere
With
nickel(II) nitrate hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen; sodium hydride; triethylamine; copper dichloride;
In
methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
3: |Glaser Coupling;
DOI:10.1039/c3gc40872h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 60 °C / Inert atmosphere
2: triethylamine; copper dichloride; nickel(II) nitrate hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen / methanol / 1.5 h / 120 °C / 760.05 Torr / Inert atmosphere
With
nickel(II) nitrate hexahydrate; N,N,N,N,-tetramethylethylenediamine; oxygen; sodium hydride; triethylamine; copper dichloride;
In
methanol; N,N-dimethyl-formamide; mineral oil;
2: |Glaser Coupling;
DOI:10.1039/c3gc40872h
