C₃₉H₄₈O₄Si

Base Information

Chemical Name:C₃₉H₄₈O₄Si
CAS No.:1401872-22-7
Molecular Formula:C₃₉H₄₈O₄Si
Molecular Weight:608.893
Hs Code.:

C<sub>39</sub>H<sub>48</sub>O<sub>4</sub>Si

Synonyms:C₃₉H₄₈O₄Si

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Chemical Property of C₃₉H₄₈O₄Si

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Technology Process of C₃₉H₄₈O₄Si

There total 5 articles about C₃₉H₄₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1401872-16-9
(4R,5S)-5-(benzyloxy)-8-[(4-methoxybenzyl)oxy]oct-1-en-4-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1401872-22-7
C₃₉H₄₈O₄Si

Guidance literature:: (4R,5S)-5-(benzyloxy)-8-[(4-methoxybenzyl)oxy]oct-1-en-4-ol; With 1H-imidazole; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

tert-butylchlorodiphenylsilane; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/hlca.201200064

Reference yield:

: 1380510-77-9
C₁₉H₂₈O₄

: 1401872-22-7
C₃₉H₄₈O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 6 h / 20 °C / Inert atmosphere

2.1: acetic acid / water / 12 h / 20 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

5.1: copper(l) iodide / tetrahydrofuran / 0.17 h / Inert atmosphere

5.2: 1 h / -20 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6.2: 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; copper(l) iodide; sodium hydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/hlca.201200064

Reference yield:

: 942137-19-1
(2R)-2-[(1S)-1-(benzyloxy)-3-butenyl]-1,4-dioxaspiro[4.5]decane

: 1401872-22-7
C₃₉H₄₈O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran; cyclohexene / 3 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 6 h / 20 °C / Inert atmosphere

3.1: acetic acid / water / 12 h / 20 °C

4.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

4.2: 4 h / 20 °C / Inert atmosphere

5.1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

6.1: copper(l) iodide / tetrahydrofuran / 0.17 h / Inert atmosphere

6.2: 1 h / -20 °C / Inert atmosphere

7.1: 1H-imidazole / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.2: 12 h / 20 °C / Inert atmosphere

With 1H-imidazole; copper(l) iodide; dimethylsulfide borane complex; sodium hydride; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; cyclohexene;
DOI:10.1002/hlca.201200064