3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

Base Information

Chemical Name:3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl
CAS No.:1423140-33-3
Molecular Formula:C₂₂H₁₈F₄O₂S
Molecular Weight:422.443
Hs Code.:

Synonyms:3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

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Chemical Property of 3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

Chemical Property:

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Technology Process of 3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

There total 4 articles about 3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1423140-32-2
(3'-(benzyloxy)-6-fluoro-4-methyl-[1,1'-biphenyl]-3-yl)(2,2,2-trifluoroethyl)sulfane

: 1423140-33-3
3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 2h;

Reference yield:

: 591-20-8
3-Bromophenol

: 1423140-33-3
3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 15 h / Reflux

3: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 53087-13-1
3-(benzyloxy)phenyl bromide

: 1423140-33-3
3'-(benzyloxy)-2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)sulfinyl)-1,1'-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; water / 15 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; water;