diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

Base Information

Chemical Name:diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate
CAS No.:1426083-85-3
Molecular Formula:C₂₅H₃₇NO₇
Molecular Weight:463.571
Hs Code.:

Synonyms:diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

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Chemical Property of diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

Chemical Property:

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Technology Process of diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

There total 4 articles about diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1426083-84-2
2-bromo-1-[4-(8-hydroxyoctyl)phenyl]ethanone

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 1426083-85-3
diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

Guidance literature:: With caesium carbonate; In acetonitrile; for 5h; Reflux;

Reference yield:

: 10472-97-6
8-phenyloctan-1-ol

: 1426083-85-3
diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0 - 20 °C

2: caesium carbonate / acetonitrile / 5 h / Reflux

With aluminum (III) chloride; caesium carbonate; In dichloromethane; acetonitrile;

Reference yield:

: 13433-00-6
diethyl aminomalonate hydrochloride

: 1426083-85-3
diethyl 2-acetamido-2-(2-(4-(8-hydroxyoctyl)phenyl)-2-oxoethyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: caesium carbonate / acetonitrile / 5 h / Reflux

With caesium carbonate; triethylamine; In dichloromethane; acetonitrile;