4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

Base Information

Chemical Name:4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl
CAS No.:945540-18-1
Molecular Formula:C₂₅H₃₁N₃O₃
Molecular Weight:421.539
Hs Code.:

Synonyms:4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

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Chemical Property of 4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

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Technology Process of 4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

There total 4 articles about 4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2-(4-aminomethylphenyl)benzamide hydrochloride

: 15026-80-9
N-pentanoylaminocyclopentane-1-carboxylic acid

: 945540-18-1
4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In dichloromethane; for 4.5h; Heating;
DOI:10.1055/S-2007-977458

Reference yield: 65.0%

: 866946-42-1
2-(4-aminomethylphenyl)benzamide

: 15026-80-9
N-pentanoylaminocyclopentane-1-carboxylic acid

: 945540-18-1
4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In acetone; at 25 - 32 ℃; for 24h; Product distribution / selectivity;

Reference yield:

: 2-(4'-aminomethylphenyl)benzonitrile hydrogen chloride

: 945540-18-1
4-[(α-N-pentanoylamino)cyclopentamidomethyl]-2'-carboxamidobiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia / dichloromethane; water / 25 - 30 °C / pH 9.0 - 9.5

2.1: potassium hydroxide; tert-butyl alcohol / 70 - 75 °C

2.2: 1 h / 2 - 5 °C / pH 1.2 - 1.4

3.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / dichloromethane / 6 h / 25 - 33 °C

With potassium hydroxide; ammonia; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; tert-butyl alcohol; In dichloromethane; water;