1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

Base Information

Chemical Name:1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate
CAS No.:1186124-18-4
Molecular Formula:C₅₀H₅₀ClN₇O₈
Molecular Weight:912.442
Hs Code.:

Synonyms:1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

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Chemical Property of 1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

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Technology Process of 1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

There total 7 articles about 1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 947331-10-4
2-butyl-4-chloro-1-((2'-(2-trityl-2H-tetrazol-5-yl)[biphenyl]-4-yl)methyl)-1H-imidazole-5-carboxylic acid

: 1186124-15-1
(5R)-5-(nitrooxy)hexyl 1-chloroethyl carbonate

: 1186124-18-4
1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;

Reference yield:

: C₆H₁₃NO₄

: 1186124-18-4
1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / -78 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With pyridine; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1186124-17-3
(5R)-5-(nitrooxy)hexyl 4-nitrobenzoate

: 1186124-18-4
1-[({[(R)-5-(nitrooxy)hexyl]oxy}carbonyl)oxy]ethyl 2-butyl-4-chloro-1-{[2'-(1H-tetrazol-5-yl)biphenyl-4-yl]methyl}-1H-imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / methanol / 1 h / 20 °C

2: pyridine / dichloromethane / -78 - 20 °C

3: caesium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

With pyridine; water; caesium carbonate; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;