methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate

Base Information

• Chemical Name: methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate
• CAS No.: 1401004-88-3
• Molecular Formula: C₂₇H₃₈N₂O₃
• Molecular Weight: 438.61
• Mol file: 1401004-88-3.mol

Synonyms:methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate

Chemical Property of methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate

There total 2 articles about methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

10-bromodecanoic acid methyl ester (26825-94-5) + 4-((4-butylphenyl)diazenyl)phenol (103939-81-7,2496-21-1) → methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate (1401004-88-3)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 24h; Inert atmosphere; Reflux;

DOI:10.1021/la3030606

Reference yield:

phenol (108-95-2,27073-41-2) → methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate (1401004-88-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 1 h / 20 °C

1.2: 5 °C

1.3: 3 h / 5 °C

2.1: potassium carbonate; potassium iodide / acetone / 24 h / Inert atmosphere; Reflux

With hydrogenchloride; potassium carbonate; potassium iodide; In water; acetone; 2.1: |Williamson Ether Synthesis;

DOI:10.1021/la3030606

Reference yield: 91.0%

methyl 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoate (1401004-88-3) → 10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoic acid (1401004-92-9)

Guidance literature:

With water; potassium hydroxide; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1021/la3030606

upstream raw materials:

10-bromodecanoic acid methyl ester

4-((4-butylphenyl)diazenyl)phenol

phenol

Downstream raw materials:

10-{4-[(4-butylphenyl)diazenyl]phenoxy}decanoic acid