[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Base Information

Chemical Name:[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester
CAS No.:934548-15-9
Molecular Formula:C₂₂H₂₅Cl₂N₃O₅
Molecular Weight:482.364
Hs Code.:

Synonyms:[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Suppliers and Price of [2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

There total 3 articles about [2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 934548-23-9
N-(chloromethyloxycarbonyl)glycine diethylamide

: 15307-79-6
diclofenac sodium

: 934548-15-9
[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Guidance literature:: With tetrabutylammomium bromide; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1002/ardp.200600145

Reference yield:

: 500871-60-3
tert-butyl (2-(diethylamino)-2-oxoethyl)carbamate

: 934548-15-9
[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / CF₃COOH / CH₂Cl₂ / 0.5 h / 20 °C

2: 45 percent / CH₂Cl₂ / -10 - 20 °C

3: 13 percent / tetrabutylammonium bromide; Et₃N / tetrahydrofuran / 24 h / 20 °C

With tetrabutylammomium bromide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.200600145

Reference yield:

: 34105-57-2
2-amino-N,N-diethylacetamide

: 934548-15-9
[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / CH₂Cl₂ / -10 - 20 °C

2: 13 percent / tetrabutylammonium bromide; Et₃N / tetrahydrofuran / 24 h / 20 °C

With tetrabutylammomium bromide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ardp.200600145