(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

Base Information

Chemical Name:(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide
CAS No.:1613465-38-5
Molecular Formula:C₂₀H₂₃N₅O₃
Molecular Weight:381.434
Hs Code.:

Synonyms:(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

Chemical Property:

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Technology Process of (E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

There total 6 articles about (E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1613465-81-8
tert-butyl ethyl(2-(methyl((6-nitro-4-oxo-3-phenyl-3,4-dihydroquinazolin-2-yl)methyl)amino)ethyl)carbamate

: 1613465-38-5
(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.75h;

Reference yield:

: 616-79-5
2-amino-5-nitro-benzoic acid

: 1613465-38-5
(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: trichlorophosphate / acetonitrile / 0.25 h / 150 °C / Inert atmosphere; Microwave irradiation

3: potassium carbonate; potassium iodide / acetonitrile / 0.17 h / 80 °C / Microwave irradiation

4: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

With potassium carbonate; triethylamine; trifluoroacetic acid; potassium iodide; trichlorophosphate; In dichloromethane; acetonitrile;

Reference yield:

: 52692-81-6
2-(chloromethyl)-6-nitro-3-phenylquinazolin-4(3H)-one

: 1613465-38-5
(E)-2-((1-ethyl-4-methylpiperazin-2-ylidene)amino)-5-nitro-N-phenylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetonitrile / 0.17 h / 80 °C / Microwave irradiation

2: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

With potassium carbonate; trifluoroacetic acid; potassium iodide; In dichloromethane; acetonitrile;